After I built my tanks, I didn't have any leaks. But several years later, when I was ready to begin plumbing the tanks to the fuselage, I pulled the sender cover plates so I could check the pickup tubes (mine were prosealed in before Van ever issued his AD). I used the cork gasket with fuel lube and the first time I had an issue with forgetting to lube the screws. This time, one of my tanks refused to hold air at all until I realized I had forgotten to tighten the screws back down. Silly me, I had tightened at four cardinal points and gotten distracted before tightening the other eight. Once they were tightened, the balloon stayed up.
On the other tank, I uncovered a pinhole leak in one of the end flanges where a rib flute wasn't filled completely. I resorted to putting the tank in our bathtub to locate this one. A tiny drill bit, toothpick and cleaner, followed by a dab of proseal packed in the opening fixed this leak in no time.
By the way, has anyone else used the balloon method to test their pitot/static connections (less instruments, of course)? It seemed to work just fine for me.